関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Homoserine lactone hydrobromide | HCID 73508 | — |
| 溶媒 | Acetic Acid | HCID 176 | — |
| 溶媒 | Hydrogen Bromide | HCID 260 | — |
| 生成物 | 2-Amino-4-bromobutanoic acid hydrobromide | HCID 13877992 | 64% |
反応手順
A suspension of α-amino-γ-butyrolactone hydrobromide in 30% HBr in HOAc was heated at 100° C. in a sealed tube for 5 days. The mixture was concentrated to give a white solid that was washed with Et2O to provide 23.1 g (64%) of 2-amino-4-bromo-butyric acid hydrobromide.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US08552205B2 |
|---|
| 出典データセット | uspto-grants-2013_10 |
|---|
| ORD ID | ord-f38f179cf9dd4131a13e1590a509ceb1 |
|---|
| 出典メモ | uspto-grants-2013_10 |
|---|
