反応式
C1C2C(=CC=CC=2)CCC1.[C:11]1([C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][C:18]=2S)[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1>>[C:11]1([C:17]2[CH:18]=[CH:19][CH:20]=[CH:21][CH:22]=2)[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1参加物
3
反応条件
- 温度
- 375 °C
実験手順
A volume of 1.5 ml of a tetralin solution containing 0.1 M of 2-phenylthiopheol was placed into 3 ml stainless-steel mini-bomb inside a dry-box. The mini-bomb was heated at 375° C. in an oven for a certain period of time and the content analyzed by GC/MS. Results in Table 1 below indicate desulfurization of 2-phenylthiophenol, giving biphenyl as the major product.
後処理
- customResults in Table 1
出典と根拠
- ORDレコード
- ord-af10a4291d544822bec950361b4f5258
- 出典データセット
- uspto-grants-2013_10
- 特許番号
- US08557101B2
関連ノート
読み込み中…