Nitric Acid → HCID 178512968、化合物

HRID 1046712

反応式

HRID 1046712 の反応式
[N+:1]([O-:4])([OH:3])=[O:2].[NH2:5][C:6](=[NH:13])[NH:7][CH2:8][CH2:9][CH2:10][CH2:11][NH2:12].[N+:14]([O-:17])([OH:16])=[O:15].[NH2:18][C:19](=[NH:26])[NH:20][CH2:21][CH2:22][CH2:23][CH2:24][NH2:25]>O>[N+:1]([O-:4])([OH:3])=[O:2].[N+:14]([O-:17])([OH:16])=[O:15].[NH2:13][C:6](=[NH:5])[NH:7][CH2:8][CH2:9][CH2:10][CH2:11][NH2:12].[N+:1]([O-:4])([OH:3])=[O:2].[N+:1]([O-:4])([OH:3])=[O:2].[N+:1]([O-:4])([OH:3])=[O:2].[NH2:26][C:19](=[NH:18])[NH:20][CH2:21][CH2:22][CH2:23][CH2:24][NH2:25]

参加物

6

反応物 3

HCID 944Nitric AcidHCID 178512945HCID 178512945、化合物HCID 178512967HCID 178512967、化合物

生成物 2

HCID 178512968HCID 178512968、化合物HCID 178512969HCID 178512969、化合物

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

Applicants have cost-effectively synthesized Agmatine Nitrate by combining nitric acid and Agmatine, mixing with water, and leaving to crystallize. Further nitratization can take place, yielding Agmatine Dinitrate or Agmatine Trinitrate. An alternative implementation comprises using Nitrous Acid (HNO2) instead of Nitric Acid (HNO3), thus yielding Agmatine Nitrite. Agmatine Nitrite has the same effects as Agmatine Nitrate, the only difference being that it requires one less step to yield Nitric Oxide (NO—). Mixed salts may also be used, such as in the non-limiting example of Agmatine Nitrate-Orotate.

後処理

  1. customleaving
  2. customto crystallize

出典と根拠

ORDレコード
ord-8d4cc6dac4a546d6b7a31875457f3f53
出典データセット
uspto-grants-2013_10
特許番号
US08569368B2

関連ノート

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