Nitric Acid → Norvaline Dinitrate

HRID 1046719

反応式

HRID 1046719 の反応式
[N+:1]([O-:4])([OH:3])=[O:2].[NH2:5][C@H:6]([C:10]([OH:12])=[O:11])[CH2:7][CH2:8][CH3:9].[N+:13]([O-:16])([OH:15])=[O:14].[NH2:17][C@H:18]([C:22]([OH:24])=[O:23])[CH2:19][CH2:20][CH3:21]>O>[N+:1]([O-:4])([OH:3])=[O:2].[N+:13]([O-:16])([OH:15])=[O:14].[NH2:5][C@H:6]([C:10]([OH:12])=[O:11])[CH2:7][CH2:8][CH3:9].[N+:1]([O-:4])([OH:3])=[O:2].[N+:1]([O-:4])([OH:3])=[O:2].[N+:1]([O-:4])([OH:3])=[O:2].[NH2:17][C@H:18]([C:22]([OH:24])=[O:23])[CH2:19][CH2:20][CH3:21]

参加物

6

反応物 3

HCID 944Nitric AcidHCID 65098L-NorvalineHCID 86628854HCID 86628854、化合物

生成物 2

HCID 86628852Norvaline DinitrateHCID 86628853Norvaline Trinitrate

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

Applicants have cost-effectively synthesized Norvaline Nitrate by combining nitric acid and Norvaline, mixing with water, and leaving to crystallize. Further nitratization can take place, yielding Norvaline Dinitrate or Norvaline Trinitrate. An alternative implementation comprises substituting Nitrous Acid (HNO2) for Nitric Acid (HNO3), thus yielding Norvaline Nitrite. Norvaline Nitrite has the same effects as Norvaline Nitrate, the only difference being that it requires one less step to yield Nitric Oxide (NO—). Mixed salts may also be used, such as in the non-limiting example of Norvaline Nitrate-Orotate.

後処理

  1. customleaving
  2. customto crystallize

出典と根拠

ORDレコード
ord-e2447ebd61824732b11dd5c1c13e1c4b
出典データセット
uspto-grants-2013_10
特許番号
US08569369B2

関連ノート

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