反応式
[N-:1]=[N+:2]=[N-:3].[Na+].[Cl-].[CH2:6]([Al+:10][CH2:11][CH:12]([CH3:14])[CH3:13])[CH:7]([CH3:9])[CH3:8]>C1(C)C=CC=CC=1>[N-:1]=[N+:2]=[N-:3].[CH2:6]([Al+:10][CH2:11][CH:12]([CH3:14])[CH3:13])[CH:7]([CH3:9])[CH3:8]参加物
4
実験手順
1.235 g of granular sodium azide (19 mmol) are added to a cold solution of diisobutyl aluminium chloride (19 mmol, 1.8M in toluene) diluted in 5 ml of toluene and the mixture is stirred at room temperature over the night to give diisobutyl aluminium azide.
出典と根拠
- ORDレコード
- ord-64e4130e48684bdfb9deb439bc89815c
- 出典データセット
- uspto-grants-2013_10
- 特許番号
- US08569528B2
関連ノート
読み込み中…