Sodium Sulfate → Molecular sieve

HRID 1052332

反応式

HRID 1052332 の反応式
S([O-])([O-])(=O)=O.[Na+:6].[Na+].[Si:8]([O-])([O-:11])([O-:10])[O-:9].[Na+].[Na+].[Na+].[Na+].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[Al+3:27].[K+]>O>[O-:10][Si:8]([O-:11])=[O:9].[O-:10][Si:8]([O-:11])=[O:9].[Na+:6].[Al+3:27]

参加物

5

反応物 3

HCID 24436Sodium SulfateHCID 24856Potassium Alum3 回HCID 26051Sodium orthosilicate2 回

生成物 1

HCID 19758701Molecular sieve

試薬・触媒・溶媒 1

HCID 962Water溶媒

反応条件

温度
55 °C

実験手順

The sodium aluminosilicate of Example 44 was prepared as follows. Approximately 300 L of hot process water and 12.4 kg of anhydrous sodium sulfate were added to a 1200-L reactor. While mixing, the reactor contents were heated to 55° C., and 5.9 L of sodium silicate were added to the reactor and mixed. A 25-min simultaneous addition step with alum and silicate solution followed, using a sodium silicate addition rate of 19.9 L/min and an alum addition rate of 7.26 L/min. After the simultaneous addition step, a reduced alum flow rate (1-2 L/min) was used to bring the batch pH to about 5.3. After digesting the batch for 10 min, the product slurry was washed and filtered using a press filter. The filtered cake was collected. A portion of filtered cake was spray dried and hammer milled to an average 5-6 micron particle size.

後処理

  1. additionWhile mixing
  2. additionmixed
  3. additionAfter the simultaneous addition step
  4. customfor 10 min
  5. washthe product slurry was washed
  6. filtrationfiltered
  7. filtrationfilter
  8. customThe filtered cake was collected
  9. customdried
  10. customhammer milled to an average 5-6 micron particle size

出典と根拠

ORDレコード
ord-134a2860ff6349ba868987c8fe7ddd28
出典データセット
uspto-grants-2016_07
特許番号
US09388299B2

関連ノート

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