Aniline → N-Phenylphthalimide

反応式

[C:1]1(=[O:11])[O:6][C:4](=O)[C:3]2=[CH:7][CH:8]=[CH:9][CH:10]=[C:2]12.[NH2:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1>>[C:13]1([N:12]2[C:1](=[O:11])[C:2]3=[CH:10][CH:9]=[CH:8][CH:7]=[C:3]3[C:4]2=[O:6])[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1

参加物

反応物 2

HCID 6115Aniline

HCID 6811Phthalic Anhydride

生成物 1

HCID 68215N-Phenylphthalimide

実験手順

1.48 g of phthalic anhydride and 0.931 g of aniline were mixed under cooling with ice, and the mixture was reacted at a temperature of 180° C. for 2 hours.

後処理

temperatureunder cooling with ice
customthe mixture was reacted at a temperature of 180° C. for 2 hours

出典と根拠

ORDレコード: ord-94fff27add5c489bbbac148b4f2c0138
出典データセット: uspto-grants-2003_02
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US06515129B1

反応ノート

読み込み中…