HCID 18667575、化合物 → HCID 18667520、化合物
反応式
[CH3:1][O:2][C:3]1[C:4]([C:9]2[CH:10]=[C:11]([N+:15]([O-])=O)[CH:12]=[CH:13][CH:14]=2)=[N:5][CH:6]=[CH:7][CH:8]=1>C(O)C.[Pd]>[CH3:1][O:2][C:3]1[C:4]([C:9]2[CH:10]=[C:11]([CH:12]=[CH:13][CH:14]=2)[NH2:15])=[N:5][CH:6]=[CH:7][CH:8]=1参加物
4
実験手順
A suspension of 3-(3-methoxypyridin-2-yl)nitrobenzene (0.391 g) in ethanol (8 ml) was hydrogenated over palladium on carbon (10% w/w, 50% wet, 120 mg) under a hydrogen atmosphere for 3 hours. The catalyst was filtered off, and the filtrate was evaporated under reduced pressure to give 3-(3-methoxypyridin-2-yl)aniline (0.34 g).
後処理
- filtrationThe catalyst was filtered off
- customthe filtrate was evaporated under reduced pressure
出典と根拠
- ORDレコード
- ord-6ed772560f014daaac142e942e0f4e3d
- 出典データセット
- uspto-grants-2003_02
- 特許番号
- US06521643B1
反応ノート
読み込み中…