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p-Toluenesulfonic acid → N-(2,3-dihydroxypropoxy)-3,4-difluoro-2-(2-fluoro-4-iodoanilino)benzamide

HRID 1062293
ノート
印刷プレビュー

反応式

HRID 1062293 の反応式
CC1(C)[O:6][CH:5]([CH2:7][O:8][NH:9][C:10](=[O:28])[C:11]2[CH:16]=[CH:15][C:14]([F:17])=[C:13]([F:18])[C:12]=2[NH:19][C:20]2[CH:25]=[CH:24][C:23]([I:26])=[CH:22][C:21]=2[F:27])[CH2:4][O:3]1.C1(C)C=CC(S(O)(=O)=O)=CC=1>CO.O.C(O)C>[OH:6][CH:5]([CH2:4][OH:3])[CH2:7][O:8][NH:9][C:10](=[O:28])[C:11]1[CH:16]=[CH:15][C:14]([F:17])=[C:13]([F:18])[C:12]=1[NH:19][C:20]1[CH:25]=[CH:24][C:23]([I:26])=[CH:22][C:21]=1[F:27]
参加物実験手順後処理出典と根拠反応ノート

参加物

6

反応物 2

HCID 6101p-Toluenesulfonic acidHCID 22061666N-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-3,4-difluoro-2-(2-fluoro-4-iodo-phenylamino)-benzamide

生成物 1

HCID 10206158N-(2,3-dihydroxypropoxy)-3,4-difluoro-2-(2-fluoro-4-iodoanilino)benzamide収率 46.1%

試薬・触媒・溶媒 3

HCID 702Ethanol溶媒HCID 887Methanol溶媒
HCID 962
Water
溶媒

実験手順

To a stirring solution of N-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-3,4-difluoro-2-(2-fluoro-4-iodo-phenylamino)-benzamide (0.907 g, 1.74 mmol) in methanol (10 mL) and water (1 mL) at ambient temperature was added p-toluene sulfonic acid (0.032 g, 0.17 mmol). After stirring for 18 hours the reaction mixture was concentrated in vacuo and the affording residue was partitioned between ethyl acetate and water. The organic layers were washed twice with water and once with saturated brine solution. Organic layers were collected, dried over Na2SO4, filtered and concentrated in vacuo affording a light brown solid, which was dissolved in ethanol and precipitated with water to afford N-(2,3-dihydroxy-propoxy)-3,4-difluoro-2-(2-fluoro-4-iodo-phenylamino)-benzamide as a white solid (0.387 g). m.p.=83-85° C.; 1NMR (400 MHz, DMSO-d6) 11.87 (s, 1H), 8.69 (s, 1H), 7.56 (d, 1H, J=11.0), 7.33-7.39 (m, 2H), 7.19 (dd, 1H, J=16.6, 9.0), 6.62-6.68 (cm, 1H), 4.82 (d, 1H, J=4.2), 4.58 (t, 1H, J=5.5), 3.84-3.87 (m, 1H), 3.66-3.72 (m, 2H), 3.3 (2H, partially hidden by HDO); MS(APCI+)=483.0; Anal.calcd/found for C16H14F3IN2O4.0.3 H2O: C, 39.41/39.02; H, 3.02/2.93; N, 5.75, 5.81; F, 11.69/11.68.

後処理

  1. concentrationwas concentrated in vacuo
  2. customthe affording residue was partitioned between ethyl acetate and water
  3. washThe organic layers were washed twice with water and once with saturated brine solution
  4. customOrganic layers were collected
  5. dry with materialdried over Na2SO4
  6. filtrationfiltered
  7. concentrationconcentrated in vacuo
  8. customaffording a light brown solid, which
  9. customprecipitated with water

出典と根拠

ORDレコード
ord-fc6a851df1fd48f9b2cc769e1ff42c09
出典データセット
uspto-grants-2005_11
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US06960614B2

反応ノート

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