Water → 3-Allyloxy-4,6-diacetyl-N-ethylaniline
反応式
[CH2:1](Br)[CH:2]=[CH2:3].[C:5]([C:8]1[CH:13]=[C:12]([C:14](=[O:16])[CH3:15])[C:11]([OH:17])=[CH:10][C:9]=1[NH:18][CH2:19][CH3:20])(=[O:7])[CH3:6].C(=O)([O-])[O-].[K+].[K+].O>CN(C)C=O>[CH2:1]([O:17][C:11]1[CH:10]=[C:9]([C:8]([C:5](=[O:7])[CH3:6])=[CH:13][C:12]=1[C:14](=[O:16])[CH3:15])[NH:18][CH2:19][CH3:20])[CH:2]=[CH2:3]参加物
6
実験手順
Allyl bromide (2 g) was added to a stirred solution of 4,6-diacetyl-3-ethylaminophenol (0.016 M) in dimethylformamide (30 ml) containing potassium carbonate (2 g). The mixture was heated at 60°-70° C. for two hours, and was then poured into water (100 ml), stirred, and the precipitated product isolated by filtration. Yield 93%, mp 82°-83° C.
後処理
- temperatureThe mixture was heated at 60°-70° C. for two hours
- customthe precipitated product isolated by filtration
出典と根拠
- ORDレコード
- ord-14afaa25679748c0adaa060c08284d90
- 出典データセット
- uspto-grants-1982_05
- 特許番号
- US04328341
反応ノート
読み込み中…