2,3-Dichloro-5,6-dicyano-1,4-benzoquinone → 5-(4-Phenylmercapto-butoxy)-carbostyril

反応式

[C:1]1([S:7][CH2:8][CH2:9][CH2:10][CH2:11][O:12][C:13]2[CH:22]=[CH:21][CH:20]=[C:19]3[C:14]=2[CH2:15][CH2:16][C:17](=[O:23])[NH:18]3)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.ClC1C(=O)C(C#N)=C(C#N)C(=O)C=1Cl>>[C:1]1([S:7][CH2:8][CH2:9][CH2:10][CH2:11][O:12][C:13]2[CH:22]=[CH:21][CH:20]=[C:19]3[C:14]=2[CH:15]=[CH:16][C:17](=[O:23])[NH:18]3)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

参加物

反応物 2

HCID 67752,3-Dichloro-5,6-dicyano-1,4-benzoquinone

HCID 542669625-(4-Phenylmercapto-butoxy)-3,4-dihydro-carbostyril

生成物 1

HCID 538402795-(4-Phenylmercapto-butoxy)-carbostyril

実験手順

Prepared analogous to Example 86 from 5-(4-phenylmercapto-butoxy)-3,4-dihydro-carbostyril and 2,3-dichloro-5,6-dicyano-benzoquinone.

出典と根拠

ORDレコード: ord-b170220e12354596aa693f80c98cfc63
出典データセット: uspto-grants-1982_05
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04329347

反応ノート

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