Methyl atropate → Methyl phenylglyoxalate

HRID 1065740

反応式

HRID 1065740 の反応式
[C:1]([O:11][CH3:12])(=[O:10])[C:2]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1)=C.C(O)(=[O:31])CCCCCCC/C=C\CCCCCCCC>C(O)(=O)C>[C:2]([C:1]([O:11][CH3:12])=[O:10])(=[O:31])[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1

参加物

4

反応物 2

HCID 193334Methyl atropateHCID 445639Oleic Acid

生成物 1

HCID 84835Methyl phenylglyoxalate収率 88%

試薬・触媒・溶媒 1

HCID 176Acetic Acid溶媒

実験手順

The co-oxidation reaction was carried out in manner as described in Example 16, except that methyl atropate was used in lieu of oleic acid. As a result, acetic acid was obtained at a yield of 95% and methyl benzoylformate was obtained at a yield of 88%.

後処理

  1. customThe co-oxidation reaction

出典と根拠

ORDレコード
ord-cba2002bf722486e97dfbc4f4ed88723
出典データセット
uspto-grants-1982_05
特許番号
US04331608

関連ノート

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