反応式
[CH:1](=[C:8]([CH2:13][O:14]C(=O)C)[C:9]([O:11][CH3:12])=[O:10])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[OH-].[Na+]>CO>[CH:1](=[C:8]([CH2:13][OH:14])[C:9]([O:11][CH3:12])=[O:10])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1参加物
4
実験手順
The crude product (2.1917 g) of methyl 2-benzylidene-3-acetoxypropionate obtained in Example 13 was dissolved in 15 ml of methanol, and 84 mg (97%, 2.04 mmols) of sodium hydroxide were added thereto. The mixture was stirred at room temperature for 4 hours to form methyl 2-benzylidene-3-hydroxypropionate.
出典と根拠
- ORDレコード
- ord-c62619cd183b43d4b504d2fff2143bda
- 出典データセット
- uspto-grants-2001_06
- 特許番号
- US06242635B1
関連ノート
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