4-Ethoxybenzoic acid → 3-BROMO-4-ETHOXYBENZOIC ACID
反応式
[CH2:1]([O:3][C:4]1[CH:12]=[CH:11][C:7]([C:8]([OH:10])=[O:9])=[CH:6][CH:5]=1)[CH3:2].[Br:13]Br>C(Cl)(Cl)Cl>[Br:13][C:5]1[CH:6]=[C:7]([CH:11]=[CH:12][C:4]=1[O:3][CH2:1][CH3:2])[C:8]([OH:10])=[O:9]参加物
4
実験手順
To a solution of 4ethoxybenzoic acid (3.6 g, 0.022 mol) in chloroform (60 ml) was added bromine (1.13 ml, 0.022 mol) in chloroform (20 ml) dropwise. After stirring overnight at room temperature the precipitate was filtered off and dried to afford the title compound as a white solid.
後処理
- filtrationwas filtered off
- customdried
出典と根拠
- ORDレコード
- ord-f98146b56e02444fa978c9f341886fd9
- 出典データセット
- uspto-grants-2001_06
- 特許番号
- US06248754B1
反応ノート
読み込み中…