Guanidine Hydrochloride → HCID 178502883、化合物
反応式
CO[N:3]1[C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[CH:5]=[C:4]1[C:12]([O:14]C)=O.[ClH:16].[NH2:17][C:18]([NH2:20])=[NH:19].[CH3:21][O-:22].[Na+]>CO>[ClH:16].[CH3:21][O:22][NH:19][C:18]([NH2:20])=[N:17][C:12]([C:4]1[NH:3][C:11]2[C:6]([CH:5]=1)=[CH:7][CH:8]=[CH:9][CH:10]=2)=[O:14]参加物
5
実験手順
The reaction was carried out in a manner similar to Example 1 except for using 0.46 g (2.24 mmol) of methyl 1-methoxy-2-indolecarboxylate, 2.14 g (22.4 mmol) of guanidine hydrochloride and 15 ml of a methanol solution of 1.21 g (22.4 mmol) of sodium methoxide. Thus 0.15 g (24.9%) of 1-methoxy-2-indoloylguanidine hydrochloride was obtained.
出典と根拠
- ORDレコード
- ord-aa527bd871fb4916971764163de8a924
- 出典データセット
- uspto-grants-2001_06
- 特許番号
- US06248772B1
反応ノート
読み込み中…