反応式
N1C=CC=CC=1.[CH2:7](Cl)[C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1.[Cl:15][SiH:16]([Cl:18])[Cl:17]>>[CH2:7]([Si:16]([Cl:18])([Cl:17])[Cl:15])[C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1参加物
4
実験手順
In the same apparatus and procedure as Example 1 above, 0.08 g (1.0 mmol) of pyridine, 0.63 g (5.0 mmol) of benzyl chloride, and 3.41 g (25.2 mmol) of trichlorosilane were reacted at 200° C. for 6 hrs. The resulting mixture was distilled to give 0.12 g of benzyltrichlorosilane (yield; 11%).
後処理
- distillationThe resulting mixture was distilled
出典と根拠
- ORDレコード
- ord-742d3d2df58f4c96b4dbd7fc7f874d68
- 出典データセット
- uspto-grants-2001_06
- 特許番号
- US06251057B1
関連ノート
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