4-hydroxy-3-(4-methoxyphenyl)benzyl Alcohol → HCID 22391344、化合物
反応式
[OH:1][C:2]1[CH:9]=[CH:8][C:5]([CH2:6][OH:7])=[CH:4][C:3]=1[C:10]1[CH:15]=[CH:14][C:13]([O:16][CH3:17])=[CH:12][CH:11]=1>CC(C)=O.O=[Mn]=O>[OH:1][C:2]1[CH:9]=[CH:8][C:5]([CH:6]=[O:7])=[CH:4][C:3]=1[C:10]1[CH:15]=[CH:14][C:13]([O:16][CH3:17])=[CH:12][CH:11]=1参加物
4
実験手順
A solution of 4-hydroxy-3-(4-methoxyphenyl)benzyl alcohol (5.54 g, 24 mmol) in acetone (250 mL) was treated with MnO2 and the mixture stirred for 3 days. The solid was filtered on diatomaceous earth and the filtrate was concentrated under reduced pressure to afford 5.96 g of title compound as a pale green oil, impure with manganese salts.
後処理
- filtrationThe solid was filtered on diatomaceous earth
- concentrationthe filtrate was concentrated under reduced pressure
出典と根拠
- ORDレコード
- ord-32ec564693d64658a2e3e46e021b33f4
- 出典データセット
- uspto-grants-2005_06
- 特許番号
- US06908935B2
反応ノート
読み込み中…