化工社化工社 化学情報印刷レポート · 研究参考用
Dibutylstannane → Bis[2-(2-ethylhexanoyloxy)ethyl]dibutyltin
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dibutylstannane | HCID 6513 | — |
| 反応物 | Vinyl 2-ethylhexanoate | HCID 62343 | — |
| 溶媒 | Cyclohexane | HCID 8078 | — |
| 生成物 | Bis[2-(2-ethylhexanoyloxy)ethyl]dibutyltin | HCID 14512235 | — |
反応手順
2.349 g (0.01 mol) of dibutyltin dihydride, 3.405 g (0.02 mol) of distilled vinyl 2-ethylhexanoate and 2.5 g of anhydrous cyclohexane were introduced into a Pyrex® tube. The exposure to ultraviolet rays was for 8 hours 30 min at 30°-35° C. The solvent was removed under vacuum at ambient temperature.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04970115 |
| 出典データセット | uspto-grants-1990_11 |
| ORD ID | ord-afdeea21f83649c98c3d79d9bf899067 |
| 出典メモ | uspto-grants-1990_11 |