反应详情

2.349 g (0.01 mol) of dibutyltin dihydride, 3.405 g (0.02 mol) of distilled vinyl 2-ethylhexanoate and 2.5 g of anhydrous cyclohexane were introduced into a Pyrex® tube. The exposure to ultraviolet rays was for 8 hours 30 min at 30°-35° C. The solvent was removed under vacuum at ambient temperature.

1. customThe solvent was removed under vacuum at ambient temperature