Methyldichlorosilane → Silane, dichlorodecylmethyl-
反応式
[CH3:1][SiH:2]([Cl:4])[Cl:3].[CH2:5]=[CH:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14]>[H+].[H+].Cl[Pt-2](Cl)(Cl)(Cl)(Cl)Cl.CC(O)C>[CH3:1][Si:2]([CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14])([Cl:4])[Cl:3]参加物
5
実験手順
2.25 Parts of methyl dichlorosilane, 4.04 parts of 1-decene and a solution containing about 0.0005 part of chloroplatinic acid catalyst in 0.006 part of 2-propanol were charged to a reaction vessel and heated to about 100°-120° C. for six hours. The product was vacuum distilled in 110°-114° C. at 1-3 Torr. 4.7 Parts (94% yield) of methyl decyl dichlorosilane was obtained.
後処理
- additionwere charged to a reaction vessel
- temperatureheated to about 100°-120° C. for six hours
- distillationdistilled in 110°-114° C. at 1-3 Torr
出典と根拠
- ORDレコード
- ord-173ce0ec5ef24d56bb4ee8213f144534
- 出典データセット
- uspto-grants-1983_07
- 特許番号
- US04391720
反応ノート
読み込み中…