Manganese sulfate monohydrate → Glucosamine sulfate manganese chloride

HRID 1075440

反応式

HRID 1075440 の反応式
[ClH:1].[OH:2][CH:3]1[O:11][C@H:10]([CH2:12][OH:13])[C@@H:8]([OH:9])[C@H:6]([OH:7])[C@H:4]1[NH2:5].O.[S:15]([O-:19])([O-:18])(=[O:17])=[O:16].[Mn+2:20]>O>[Cl-:1].[Mn+3:20].[S:15]([O-:19])([O-:18])(=[O:17])=[O:16].[OH:2][CH:3]1[O:11][C@H:10]([CH2:12][OH:13])[C@@H:8]([OH:9])[C@H:6]([OH:7])[C@H:4]1[NH2:5]

参加物

4

反応物 2

HCID 177577Manganese sulfate monohydrateHCID 2723635(3R,4R,5S,6R)-3-amino-6-(hydroxymethyl)oxane-2,4,5-triol hydrochloride

生成物 1

HCID 86754063Glucosamine sulfate manganese chloride

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

Example 1 was repeated using 450 g of purified water, 107.8 g (0.5 mole) of glucosamine hydrochloride and 42.3 g (0.25 mole) of manganese sulfate monohydrate instead of the sodium sulfate. After freeze drying, glucosamine sulfate manganese chloride was obtained as a white powder in a yield of 144 g (98% of theoretical).

後処理

  1. customAfter freeze drying

出典と根拠

ORDレコード
ord-045279f9fee44a129807d5810a9ab026
出典データセット
uspto-grants-1999_05
特許番号
US05902801

関連ノート

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