Formaldehyde → HCID 86733424、化合物

HRID 1076528

反応式

HRID 1076528 の反応式
C[NH:2][C:3]([N:5]([CH2:9]CC)[CH2:6][CH2:7][CH3:8])=[O:4].C=O.[NH:14]1[CH2:19][CH2:18][O:17][CH2:16][CH2:15]1>>[O:17]1[CH2:18][CH2:19][N:14]([CH2:9][N:5]([CH2:6][CH2:7][CH3:8])[C:3]([NH2:2])=[O:4])[CH2:15][CH2:16]1.[CH3:9][N:5]([CH2:6][CH2:7][CH3:8])[C:3]([NH2:2])=[O:4]

参加物

4

反応物 3

HCID 712FormaldehydeHCID 8083MorpholineHCID 215877Urea, 1,1-dipropyl-3-methyl-2 回

生成物 1

HCID 86733424HCID 86733424、化合物

実験手順

1 mol of N-methyl dipropylurea and 1 mol of formol in aqueous 30% solution are mixed. To this solution 1 mol of morpholine is slowly added while cooling. The stirring is maintained one hour after the end of the N-methyl dipropylurea addition. After evaporation to dryness a crystalline product is obtained which melts at 110°C. The yield of the reaction is 98%.

後処理

  1. temperaturewhile cooling
  2. temperatureThe stirring is maintained one hour
  3. customAfter evaporation to dryness a crystalline product
  4. customis obtained which melts at 110°C

出典と根拠

ORDレコード
ord-6cd7fcff60ed43e0b748a5001dd441f9
出典データセット
uspto-grants-1976_05
特許番号
US03957774

関連ノート

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