化工社化工社 化学情報印刷レポート · 研究参考用
Sodium Hydroxide → Perilla alcohol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | Perillyl acetate | HCID 61780 | — |
| 生成物 | Perilla alcohol | HCID 369312 | 97.7% |
反応手順
Perillyl acetate (196 g.) derived from either of the examples mentioned and 30% aqueous sodium hydroxide (60 g.) were refluxed gently with stirring for 4 hours. The oil layer was separated and distilled under reduced pressure to give perillyl alcohol (150 g.) b.P. 80°/0.7 mm., αD20 + 102.5.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US03957856 |
| 出典データセット | uspto-grants-1976_05 |
| ORD ID | ord-39ae34768f2747dca013ecfce2e00257 |
| 出典メモ | uspto-grants-1976_05 |