Methyl iodide → 3-(3-(3-Pentynyloxy)-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide
反応式
[CH3:1][I:2].[CH2:3]([O:8][C:9]1[C:13]([C:14]2[CH:15]=[N:16][CH:17]=[CH:18][CH:19]=2)=[N:12][S:11][N:10]=1)[CH2:4][C:5]#[C:6][CH3:7]>CC(C)=O>[I-:2].[CH2:3]([O:8][C:9]1[C:13]([C:14]2[CH:15]=[N+:16]([CH3:1])[CH:17]=[CH:18][CH:19]=2)=[N:12][S:11][N:10]=1)[CH2:4][C:5]#[C:6][CH3:7]参加物
4
実験手順
A mixture of methyl iodide (0.6 ml, 9 mmol) and 3-(3-(3-pentynyloxy)-1,2,5-thiadiazol-4-yl)pyridine (3 mmol) in acetone (10 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.68 g (59%).
後処理
- customThe title compound precipitated from the solution
- filtrationwas collected by filtration
- customto yield 0.68 g (59%)
出典と根拠
- ORDレコード
- ord-40edce02e5454e059c1ff1a8825955a5
- 出典データセット
- uspto-grants-1996_08
- 特許番号
- US05545638
反応ノート
読み込み中…