Triethylamine → HCID 86744708、化合物

HRID 1084800

反応式

HRID 1084800 の反応式
[CH:1](=[N:6][OH:7])[C:2]([CH3:5])([CH3:4])[CH3:3].ClN1C(=O)CCC1=O.[CH:16]([P:18](=[O:25])([O:22][CH2:23][CH3:24])[O:19][CH2:20][CH3:21])=[CH2:17].C(N(CC)CC)C>ClCCl.N1C=CC=CC=1>[C:2]([C:1]1[CH2:17][CH:16]([P:18](=[O:25])([O:22][CH2:23][CH3:24])[O:19][CH2:20][CH3:21])[O:7][N:6]=1)([CH3:5])([CH3:4])[CH3:3]

参加物

7

反応物 4

HCID 8471TriethylamineHCID 31398ChlorosuccinimideHCID 69629Diethyl vinylphosphonateHCID 136457Pivalaldoxime

生成物 1

HCID 86744708HCID 86744708、化合物

試薬・触媒・溶媒 2

HCID 1049Pyridine溶媒HCID 6344Dichloromethane溶媒

実験手順

The procedure is analogous to that of Example 25 using 15.2 g (0.15 mol) of pivalaldoxime, 22.0 g (0.165 mol) of N-chlorosuccinimide, 0.5 ml of pyridine, 27.1 g (0.165 mol) of diethyl vinylphosphonate and 22.9 ml (0.165 mol) of triethylamine in dichloromethane. The product is obtained as an oil after the usual working up.

後処理

  1. customThe product is obtained as an oil after the

出典と根拠

ORDレコード
ord-f7ff29b72e2e4375b1d0bcfc664d7b01
出典データセット
uspto-grants-1991_04
特許番号
US05006515

関連ノート

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