化工社化工社 化学情報印刷レポート · 研究参考用
Prostaglandin D2 → Arachidonic Acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Prostaglandin D2 | HCID 448457 | — |
| 反応物 | Prostaglandin E2 | HCID 5280360 | — |
| 反応物 | Dinoprost | HCID 5280363 | — |
| 反応物 | 6-Ketoprostaglandin F1 alpha | HCID 5280888 | — |
| 生成物 | Arachidonic Acid | HCID 444899 | — |
反応手順
The thus obtained acidic liquid was extracted 3 times with each 5 ml of ether, and after evaporating ether off from the ether extract, the dried solid was subjected to esterification by a diazomethane solution. The product of esterification was fractioned by thin layer chromatography while developing with a 90:50:20:100 by volume mixture of ethyl acetate, isooctane, acetic acid and water to obtained fractioned spots which were identified by the authentic specimens of PGD2, PGE2, PGF2α and 6-keto-PGF1α.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05008243 |
| 出典データセット | uspto-grants-1991_04 |
| ORD ID | ord-970a20277e544f4b819a8d970877b931 |
| 出典メモ | uspto-grants-1991_04 |