Ethanolamine → 2-(2-Methyl-2-decyl)-2-oxazoline

HRID 1086429

反応式

HRID 1086429 の反応式
[C:1]([C:3]([CH3:15])([CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12]CC)[CH3:4])#[N:2].N[CH2:17][CH2:18][OH:19]>C(O)CCC.O.O.C([O-])(=O)C.[Cd+2].C([O-])(=O)C>[CH3:15][C:3]([C:1]1[O:19][CH2:18][CH2:17][N:2]=1)([CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])[CH3:4]

参加物

5

反応物 2

HCID 700EthanolamineHCID 198259372,2-Dimethyldodecanenitrile

生成物 1

HCID 198259392-(2-Methyl-2-decyl)-2-oxazoline

試薬・触媒・溶媒 2

HCID 6537495Cadmium acetate, dihydrate触媒HCID 2631-Butanol溶媒

実験手順

100 mmoles of 2-cyano-2-methyldodecane is reacted with 120 mmoles of 2-aminoethanol in 50 ml of 1-butanol in presence of 2.5 mmoles of cadmium acetate dihydrate as outlined under Example 1 to give 2-(2-methyl-2-decyl)-2-oxazoline.

出典と根拠

ORDレコード
ord-13c2ab71246844ebb4f102233572a39d
出典データセット
uspto-grants-1991_07
特許番号
US05030629

関連ノート

読み込み中…