Hexanenitrile → HCID 178442284、化合物
反応式
[NH2:1][CH2:2][C:3]([NH2:6])([CH3:5])[CH3:4].[C:7](#N)[CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]>C(=S)=S>[CH3:4][C:3]1([CH3:5])[CH2:2][NH:1][C:7]([CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])=[N:6]1参加物
4
実験手順
8.41 g (95.4 mmoles) of 1,2-diamino-2-methylpropane, 7.4 g (76.16 mmoles) of hexanenitrile and 0.4 ml of carbon disulfide were heated at 125° C. for 24 hours and then worked up as under Example 23. Distillation at 105°-107° C./0.5 mm gave 9.4 g (73.4%) of product.
後処理
- distillationDistillation at 105°-107° C./0.5 mm
出典と根拠
- ORDレコード
- ord-774414b09cb54582b80ce98d82d5fa71
- 出典データセット
- uspto-grants-1991_07
- 特許番号
- US05030629
反応ノート
読み込み中…