Hexanenitrile → HCID 178442284、化合物

HRID 1086440

反応式

HRID 1086440 の反応式
[NH2:1][CH2:2][C:3]([NH2:6])([CH3:5])[CH3:4].[C:7](#N)[CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]>C(=S)=S>[CH3:4][C:3]1([CH3:5])[CH2:2][NH:1][C:7]([CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])=[N:6]1

参加物

4

反応物 2

HCID 12352HexanenitrileHCID 131282-Methylpropylenediamine

生成物 1

HCID 178442284HCID 178442284、化合物収率 73.4%

試薬・触媒・溶媒 1

HCID 6348Carbon Disulfide溶媒

実験手順

8.41 g (95.4 mmoles) of 1,2-diamino-2-methylpropane, 7.4 g (76.16 mmoles) of hexanenitrile and 0.4 ml of carbon disulfide were heated at 125° C. for 24 hours and then worked up as under Example 23. Distillation at 105°-107° C./0.5 mm gave 9.4 g (73.4%) of product.

後処理

  1. distillationDistillation at 105°-107° C./0.5 mm

出典と根拠

ORDレコード
ord-774414b09cb54582b80ce98d82d5fa71
出典データセット
uspto-grants-1991_07
特許番号
US05030629

関連ノート

読み込み中…