Water → Phenol, 3-amino-, sodium salt

HRID 1086937ノート

反応式

HRID 1086937 の反応式
O.[NH2:2][C:3]1[CH:4]=[C:5]([OH:9])[CH:6]=[CH:7][CH:8]=1.[OH-].[Na+:11]>C1(C)C=CC=CC=1>[NH2:2][C:3]1[CH:4]=[C:5]([O-:9])[CH:6]=[CH:7][CH:8]=1.[Na+:11]

参加物

5

反応物 3

HCID 962WaterHCID 115683-AminophenolHCID 14798Sodium Hydroxide

生成物 1

HCID 23669774Phenol, 3-amino-, sodium salt

試薬・触媒・溶媒 1

HCID 1140Toluene溶媒

実験手順

Another three-necked flask equipped with a Dean-Stark water separator, condenser, nitrogen inlet and outlet, thermometer and a mechanical stirrer is charged with 261.91 grams (2.4 moles) of meta-aminophenol, 192 grams (2.4 moles) of 50% aqueous sodium hydroxide and 720 milliliters of toluene. The mixture is heated at 100° -140° C. for three hours to remove all of the water and toluene and provide sodium meta-aminophenolate.

後処理

  1. temperatureThe mixture is heated at 100° -140° C. for three hours
  2. customto remove all of the water and toluene

出典と根拠

ORDレコード
ord-ae0f816484f14366b057ec5e98c5203f
出典データセット
uspto-grants-1991_07
特許番号
US05032668

反応ノート

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