1,3-Dibromopropane → HCID 54300370、化合物

HRID 1088422

反応式

HRID 1088422 の反応式
[CH:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[OH:10])=[CH:2][CH3:3].Br[CH2:12][CH2:13][CH2:14]Br>>[CH:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[O:10][CH2:12][CH2:13][CH2:14][O:10][C:5]1[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=1[CH:1]=[CH:2][CH3:3])=[CH:2][CH3:3]

参加物

3

反応物 2

HCID 80011,3-DibromopropaneHCID 930292-Propenylphenol

生成物 1

HCID 54300370HCID 54300370、化合物

実験手順

1,3-bis(ortho-propenylphenoxy)propane is prepared in a procedure similar to Example I, except that 537 grams (4.0 moles) of propenyl phenol is employed along with 403 grams (1.98 moles) of 1,3-dibromo-propane to produce a reaction mixture extracted with methylene chloride and dried over magnesium sulfate, then vacuum distilled to give 311 grams (50% yield) of a solid with melting point 45°-48° C.

後処理

  1. customto produce a reaction mixture
  2. extractionextracted with methylene chloride
  3. dry with materialdried over magnesium sulfate
  4. distillationvacuum distilled

出典と根拠

ORDレコード
ord-291fecb3e6064f8284170aa95bbf8f36
出典データセット
uspto-grants-1990_10
特許番号
US04962161

関連ノート

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