Benzene → Benzenamine, 4-methoxy-N-(1-phenylethylidene)-
反応式
[C:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1)(=O)[CH3:2].[CH3:10][O:11][C:12]1[CH:17]=[CH:16][C:15]([NH2:18])=[CH:14][CH:13]=1.C1C=CC=CC=1>O>[CH3:2][C:1](=[N:18][C:15]1[CH:16]=[CH:17][C:12]([O:11][CH3:10])=[CH:13][CH:14]=1)[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1参加物
5
実験手順
A solution of acetophenone (64 ml), p-anisidine (65 mg), benzene (100 ml) was refluxed in the presence of molecular sieve (100 g) with continuous removal of water. The crude product was purified by crystallizing it from ethanol to give N-(αmethyl-benzylidene)-p-anisidine (VII) (50 g). VII had a melting point of 81°-82° C.
後処理
- customThe crude product was purified
- customby crystallizing it from ethanol
出典と根拠
- ORDレコード
- ord-2a2fc40be80a4e3baeb746a53558c36c
- 出典データセット
- uspto-grants-1990_10
- 特許番号
- US04962234
反応ノート
読み込み中…