Thionyl Chloride → HCID 53411290、化合物

HRID 1089387ノート

反応式

HRID 1089387 の反応式
[Cl:1][C:2]1[CH:3]=[C:4]([CH:10]=[CH:11][CH:12]=1)[CH:5]=[CH:6][C:7](O)=[O:8].S(Cl)([Cl:15])=O>C1C=CC=CC=1>[Cl:1][C:2]1[CH:3]=[C:4]([CH:10]=[CH:11][CH:12]=1)[CH:5]=[CH:6][C:7]([Cl:15])=[O:8]

参加物

4

反応物 2

HCID 24386Thionyl ChlorideHCID 746313-(3-Chlorophenyl)prop-2-enoic acid

生成物 1

HCID 53411290HCID 53411290、化合物

試薬・触媒・溶媒 1

HCID 241Benzene溶媒

実験手順

100 ml of benzene was added to 18.3 grams of m-chlorocinnamic acid. 12 ml of thionyl chloride was added dropwise slowly thereto at ambient temperature. The temperature was elevated to 80° C. and the heating was continued until foaming ceased. Benzene and thionyl chloride were distilled off and the residue was dried thoroughly under reduced pressure.

後処理

  1. customat ambient temperature
  2. customwas elevated to 80° C.
  3. distillationBenzene and thionyl chloride were distilled off
  4. customthe residue was dried thoroughly under reduced pressure

出典と根拠

ORDレコード
ord-17f1f2c49d114d1e8fc10fad0f9b9d4b
出典データセット
uspto-grants-1990_10
特許番号
US04966694

反応ノート

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