Thionyl Chloride → Monopropyl Terephthaloyl Chloride

HRID 1089643ノート

反応式

HRID 1089643 の反応式
[CH3:1][C:2]1[CH:10]=[C:9]([C:11]([Cl:13])=[O:12])[CH:8]=[CH:7][C:3]=1[C:4]([Cl:6])=[O:5].[C:14](OCCC)(=O)[C:15]1C=CC(C([O-])=O)=CC=1.[K+].S(Cl)(Cl)=O>C1(C)C=CC=CC=1>[CH2:1]([C:2]1[CH:10]=[C:9]([C:11]([Cl:13])=[O:12])[CH:8]=[CH:7][C:3]=1[C:4]([Cl:6])=[O:5])[CH2:14][CH3:15]

参加物

5

反応物 3

HCID 24386Thionyl ChlorideHCID 22057046HCID 22057046、化合物HCID 23693908Potassium Monopropyl Terephthalate

生成物 1

HCID 19915522Monopropyl Terephthaloyl Chloride

試薬・触媒・溶媒 1

HCID 1140Toluene溶媒

実験手順

This compound was prepared by the procedure described for monomethyl terephthaloyl chloride. Typical reagent levels were as follows: potassium monopropyl terephthalate (49.0g, 0.20 mole), thionyl chloride (29.8g, 0.25 mole) and 100 ml of toluene. The product was used without further purification.

後処理

  1. customThis compound was prepared by the procedure
  2. customThe product was used without further purification

出典と根拠

ORDレコード
ord-ac7eb9e4db084883b32afbccc60fb5aa
出典データセット
uspto-grants-1992_01
特許番号
US05078907

反応ノート

読み込み中…