Thionyl Chloride → HCID 19915516、化合物

HRID 1089646ノート

反応式

HRID 1089646 の反応式
[CH3:1][C:2]1[CH:10]=[C:9]([C:11]([Cl:13])=[O:12])[CH:8]=[CH:7][C:3]=1[C:4]([Cl:6])=[O:5].[C:14](OCCCC)(=O)[C:15]1C=CC(C([O-])=O)=C[CH:16]=1.[K+].S(Cl)(Cl)=O>C1(C)C=CC=CC=1>[CH2:1]([C:2]1[CH:10]=[C:9]([C:11]([Cl:13])=[O:12])[CH:8]=[CH:7][C:3]=1[C:4]([Cl:6])=[O:5])[CH2:14][CH2:15][CH3:16]

参加物

5

反応物 3

HCID 24386Thionyl ChlorideHCID 22057046HCID 22057046、化合物HCID 23693905Potassium Monobutyl Terephthalate

生成物 1

HCID 19915516HCID 19915516、化合物

試薬・触媒・溶媒 1

HCID 1140Toluene溶媒

実験手順

This compound was prepared by the procedure described for monomethyl terephthaloyl chloride. Typical reagent levels were as follows: potassium monobutyl terephthalate (10.0 g, 0.0384 mole), thionyl chloride (4.57, 0.0384 mole) and 40 ml of toluene. The yield of product was 8.5 g (92%). This material was used without further purification.

後処理

  1. customThis compound was prepared by the procedure
  2. customThis material was used without further purification

出典と根拠

ORDレコード
ord-93af8425e7774440b21e6142f5d1b490
出典データセット
uspto-grants-1992_01
特許番号
US05078907

反応ノート

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