Thionyl Chloride → Monohexyl Terephthaloyl Chloride

HRID 1089648ノート

反応式

HRID 1089648 の反応式
[CH3:1][C:2]1[CH:10]=[C:9]([C:11]([Cl:13])=[O:12])[CH:8]=[CH:7][C:3]=1[C:4]([Cl:6])=[O:5].C(OCCCCCC)(=O)[C:15]1[CH:23]=[CH:22]C(C([O-])=O)=[CH:17][CH:16]=1.[K+].S(Cl)(Cl)=O>C1(C)C=CC=CC=1>[CH2:1]([C:2]1[CH:10]=[C:9]([C:11]([Cl:13])=[O:12])[CH:8]=[CH:7][C:3]=1[C:4]([Cl:6])=[O:5])[CH2:17][CH2:16][CH2:15][CH2:23][CH3:22]

参加物

5

反応物 3

HCID 24386Thionyl ChlorideHCID 22057046HCID 22057046、化合物HCID 23693907Potassium monohexyl terephthalate

生成物 1

HCID 19915510Monohexyl Terephthaloyl Chloride

試薬・触媒・溶媒 1

HCID 1140Toluene溶媒

実験手順

This compound was prepared by the method described for monomethyl terephthaloyl chloride. Typical reagent levels were as follows: potassium monohexyl terephthalate (18.6 g, 0.64 mole), thionyl chloride (9.21 g, 0.774 mole) and 100 ml of toluene. The product was used without further purification.

後処理

  1. customThis compound was prepared by the method
  2. customThe product was used without further purification

出典と根拠

ORDレコード
ord-5ebe672c30364d6da854725a7ce28276
出典データセット
uspto-grants-1992_01
特許番号
US05078907

反応ノート

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