2-tert-Butyl-4-methylphenol → 2-Bromo-4-methyl-6-tert-butylphenol
反応式
[Br:1]N1C(=O)CCC1=O.[C:9]([C:13]1[CH:18]=[C:17]([CH3:19])[CH:16]=[CH:15][C:14]=1[OH:20])([CH3:12])([CH3:11])[CH3:10]>CN(C)C=O>[Br:1][C:15]1[CH:16]=[C:17]([CH3:19])[CH:18]=[C:13]([C:9]([CH3:12])([CH3:11])[CH3:10])[C:14]=1[OH:20]参加物
4
実験手順
Under nitrogen atmosphere, a dimethylformamide 100 ml solution of N-bromosuccinimide (22.25 g, 125 mmol) was added dropwise at 0° C. to a dimethylformamide 100 ml solution of 2-tert-butyl-4-methylphenol (20.53 g, 125 mmol) with stirring, the resulting reaction mixture was brought up to room temperature and stirred for 5 hours.
後処理
- customthe resulting reaction mixture
- customwas brought up to room temperature
- stirringstirred for 5 hours
出典と根拠
- ORDレコード
- ord-8c1ae205379742eeba247d9b141e0fbb
- 出典データセット
- uspto-grants-2000_05
- 特許番号
- US06066704
反応ノート
読み込み中…