N-Methylacetamide → methylvinyldi-(N-methylacetamido)silane
反応式
[Na].[CH3:2][NH:3][C:4](=[O:6])[CH3:5].[CH3:7][CH:8]=[CH:9][SiH:10](Cl)Cl>C1(C)C=CC=CC=1>[CH3:7][CH:8]=[CH:9][SiH:10]([N:3]([CH3:2])[C:4](=[O:6])[CH3:5])[N:3]([CH3:2])[C:4](=[O:6])[CH3:5]参加物
5
実験手順
The acetamidosilanes can be prepared as by the following illustration: mixing a sodium salt of N-methylacetamide with methylvinyldichlorosilane in an inert organic solvent such as toluene, filtering the by-produced sodium chloride from the toluene-product solution, and thereafter removing the toluene by vacuum distillation to obtain the product, methylvinyldi(N-methylacetamido)silane.
後処理
- filtrationfiltering the by-produced sodium chloride from the toluene-product solution
- customremoving the toluene
- distillationby vacuum distillation
出典と根拠
- ORDレコード
- ord-2f59463d4e6246b7b62dc5eae742cea5
- 出典データセット
- uspto-grants-1990_12
- 特許番号
- US04978706
反応ノート
読み込み中…