Sodium Carbonate → S-[2-(5-Methyl-4-imidazolylmethylthio)ethyl]-N-cyano-N'-methylisothiourea
反応式
Cl.[CH3:2][C:3]1[NH:7][CH:6]=[N:5][C:4]=1[CH2:8][S:9][CH2:10][CH2:11][S:12][C:13](=[N:17][CH3:18])[NH:14][C:15]#[N:16].C(=O)([O-])[O-].[Na+].[Na+]>>[CH3:2][C:3]1[NH:7][CH:6]=[N:5][C:4]=1[CH2:8][S:9][CH2:10][CH2:11][S:12][C:13](=[N:17][CH3:18])[NH:14][C:15]#[N:16]参加物
3
実験手順
This hydrochloride may be treated with aqueous sodium carbonate and the mixture extracted with chloroform and the chloroform extracts evaporated to give the free base.
後処理
- extractionthe mixture extracted with chloroform
- customthe chloroform extracts evaporated
- customto give the free base
出典と根拠
- ORDレコード
- ord-ab9594230f544df3a55c302a987c182c
- 出典データセット
- uspto-grants-1978_10
- 特許番号
- US04120972
反応ノート
読み込み中…