Methyl iodide → 1-(2,6-Dichlorophenyl)-3-carbamyl-3-methylthiouronium iodide

HRID 1154295ノート

反応式

HRID 1154295 の反応式
[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([Cl:8])[C:3]=1[NH:9][C:10]([NH:12][C:13](=[O:15])[NH2:14])=[S:11].[I:16][CH3:17]>CO>[I-:16].[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([Cl:8])[C:3]=1[NH+:9]=[C:10]([N:12]([C:13](=[O:15])[NH2:14])[CH3:17])[SH:11]

参加物

4

反応物 2

HCID 6328Methyl iodideHCID 204344241-(2,6-Dichlorophenyl)-3-carbamylthiourea

生成物 1

HCID 1784851951-(2,6-Dichlorophenyl)-3-carbamyl-3-methylthiouronium iodide

試薬・触媒・溶媒 1

HCID 887Methanol溶媒

実験手順

26.4 g (0.1 mole) of 1-(2,6-dichlorophenyl)-3-carbamylthiourea is combined with 200 ml of methanol and 14.1 g (0.1 mole) of iodomethane and refluxed for 4 hours. This is then evaporated to dryness and 100 ml of hexane is added. The mixture is filtered to obtain 1-(2,6-dichlorophenyl)-3-carbamyl-3-methylthiouronium iodide.

後処理

  1. temperaturerefluxed for 4 hours
  2. customThis is then evaporated to dryness and 100 ml of hexane
  3. additionis added
  4. filtrationThe mixture is filtered

出典と根拠

ORDレコード
ord-05dcdcd27cf047b49f2e85843fe5f82a
出典データセット
uspto-grants-1984_12
特許番号
US04488993

反応ノート

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