P-Toluic Acid → 4-Methylbenzoyl Chloride

HRID 1158

反応式

HRID 1158 の反応式
[CH3:1][C:2]1[CH:10]=[CH:9][C:5]([C:6](O)=[O:7])=[CH:4][CH:3]=1.S(Cl)([Cl:13])=O>>[CH3:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([Cl:13])=[O:7])=[CH:4][CH:3]=1

参加物

3

反応物 2

HCID 7470P-Toluic AcidHCID 24386Thionyl Chloride

生成物 1

HCID 134054-Methylbenzoyl Chloride

実験手順

4-Methylbenzoyl chloride was prepared in a conventional manner from 4-methylbenzoic acid and thionyl chloride and after excess thionyl chloride was distilled off, was used as the crude product in the side chain chlorination.

後処理

  1. distillationafter excess thionyl chloride was distilled off

出典と根拠

ORDレコード
ord-4c3ca7fee7ca4cb68a75ae1c5be3919e
出典データセット
uspto-grants-1998_03
特許番号
US05723613

関連ノート

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