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Hydroxyamine hydrochloride → 2-[2-amino-5-(hydroxyimino-methyl)-6-methylsulfanyl-pyrimidin-4-ylamino]-N-(3-trifluoromethyl-phenyl)-acetamide

HRID 1160113
ノート
印刷プレビュー

反応式

HRID 1160113 の反応式
[NH2:1][C:2]1[N:7]=[C:6]([NH:8][CH2:9][C:10]([NH:12][C:13]2[CH:18]=[CH:17][CH:16]=[C:15]([C:19]([F:22])([F:21])[F:20])[CH:14]=2)=[O:11])[C:5]([CH:23]=O)=[C:4]([S:25][CH3:26])[N:3]=1.C(=O)(O)[O-].[K+].Cl.[NH2:33][OH:34]>CO>[NH2:1][C:2]1[N:7]=[C:6]([NH:8][CH2:9][C:10]([NH:12][C:13]2[CH:18]=[CH:17][CH:16]=[C:15]([C:19]([F:22])([F:21])[F:20])[CH:14]=2)=[O:11])[C:5]([CH:23]=[N:33][OH:34])=[C:4]([S:25][CH3:26])[N:3]=1
参加物反応条件実験手順後処理出典と根拠反応ノート

参加物

5

反応物 3

HCID 443297Hydroxyamine hydrochlorideHCID 516893Potassium BicarbonateHCID 111766082-(2-amino-5-formyl-6-methylsulfanyl-pyrimidin-4-ylamino)-N-(3-trifluoromethyl-phenyl)-acetamide

生成物 1

HCID 724763122-[2-amino-5-(hydroxyimino-methyl)-6-methylsulfanyl-pyrimidin-4-ylamino]-N-(3-trifluoromethyl-phenyl)-acetamide収率 29%

試薬・触媒・溶媒 1

HCID 887
Methanol
溶媒

反応条件

温度
60 °C

実験手順

To a round bottom flask was added 2-(2-amino-5-formyl-6-methylsulfanyl-pyrimidin-4-ylamino)-N-(3-trifluoromethyl-phenyl)-acetamide (50.0 mg, 0.13 mmol, 1.0 mmol), MeOH (2.0 mL), potassium bicarbonate (51.0 mg, 0.51 mmol, 4.0 eq.), and hydroxylamine HCl (35.6 mg, 0.51 mmol, 4.0 eq.). The reaction was heated to 60° C. for 72 hrs before quenching with H2O (10 mL) and EtOAc (50 mL). The EtOAc layer washed with brine, dried with Na2SO4, and concentrated to give crude 2-[2-amino-5-(hydroxyimino-methyl)-6-methylsulfanyl-pyrimidin-4-ylamino]-N-(3-trifluoromethyl-phenyl)-acetamide as an oil. The product was then precipitated out with 3 mL water and 0.5 mL of ACN, filtered and rinsed with 2 mL of (1:2 ACN: H2O) to give pure 2-[2-amino-5-(hydroxyimino-methyl)-6-methylsulfanyl-pyrimidin-4-ylamino]-N-(3-trifluoromethyl-phenyl)-acetamide as a solid (15.0 mg, 29%). LC/MSD (HP Series 1100 MSD): Expected MW: 400, Observed M+H, 401.1, Retention time: 1.48 min. ANALYTICAL HPLC: >80%, Retention time: 2.89 min (8 minute run). 1H-NMR (d6-DMSO): 10.98 (s, 1H), 10.50 (s, 1H), 8.40 (t, 1H), 8.15 (s, 1H), 8.09 (s, 1H), 7.77 (d, 1H), 7.58 (t, 1H), 7.40 (d, 1H), 5.90 (br s, 2H), 4.36 (d, 2H), 2.40 (s, 3H) ppm.

後処理

  1. custombefore quenching with H2O (10 mL) and EtOAc (50 mL)
  2. washThe EtOAc layer washed with brine
  3. dry with materialdried with Na2SO4
  4. concentrationconcentrated
  5. customto give crude 2-[2-amino-5-(hydroxyimino-methyl)-6-methylsulfanyl-pyrimidin-4-ylamino]-N-(3-trifluoromethyl-phenyl)-acetamide as an oil
  6. customThe product was then precipitated out with 3 mL water and 0.5 mL of ACN
  7. filtrationfiltered
  8. washrinsed with 2 mL of (1:2 ACN: H2O)

出典と根拠

ORDレコード
ord-ea6afff487c34b4397d49caa226cc865
出典データセット
uspto-grants-2010_10
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US07816353B2

反応ノート

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