Ammonia → 5-Chloro-2-methoxybenzene-1-sulfonamide
反応式
[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([O:12][CH3:13])=[C:6]([S:8](Cl)(=[O:10])=[O:9])[CH:7]=1.[NH3:14]>O1CCCC1>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([O:12][CH3:13])=[C:6]([S:8]([NH2:14])(=[O:10])=[O:9])[CH:7]=1参加物
4
実験手順
To a solution of 5-chloro-2-methoxybenzene sulfonyl chloride (1.0 g, 4.15 mmol) in tetrahydrofuran (10 mL) was bubbled ammonia gas until saturated. The reaction was stirred overnight. The white solid that precipitated out of solution was collected by filtration and washed with dichloromethane to give the title compound (0.52 g).
後処理
- customThe white solid that precipitated out of solution
- filtrationwas collected by filtration
- washwashed with dichloromethane
出典と根拠
- ORDレコード
- ord-f40b87c7e96a4cb98fe793f02a60727f
- 出典データセット
- uspto-grants-2006_08
- 特許番号
- US07098212B2
反応ノート
読み込み中…