1-(4-Chloro-phenyl)-2-(4-nitro-phenyl)-ethane-1,2-diamine → HCID 178494527、化合物

HRID 1167340ノート

反応式

HRID 1167340 の反応式
[OH:1][CH2:2][C:3]1[CH:4]=[C:5]([CH:8]=[C:9]([CH2:11][O:12][CH3:13])[CH:10]=1)[C:6]#[N:7].[Cl:14][C:15]1[CH:20]=[CH:19][C:18]([CH:21]([NH2:33])[CH:22]([C:24]2[CH:29]=[CH:28][C:27]([N+:30]([O-:32])=[O:31])=[CH:26][CH:25]=2)N)=[CH:17][CH:16]=1>CC#N>[Cl:14][C:15]1[CH:16]=[CH:17][C:18]([CH:21]2[NH:33][C:6]([C:5]3[CH:4]=[C:3]([CH2:2][OH:1])[CH:10]=[C:9]([CH2:11][O:12][CH3:13])[CH:8]=3)=[N:7][CH:22]2[C:24]2[CH:29]=[CH:28][C:27]([N+:30]([O-:32])=[O:31])=[CH:26][CH:25]=2)=[CH:19][CH:20]=1

参加物

4

反応物 2

HCID 227210671-(4-Chloro-phenyl)-2-(4-nitro-phenyl)-ethane-1,2-diamineHCID 229962313-Hydroxymethyl-5-methoxymethyl-benzonitrile

生成物 1

HCID 178494527HCID 178494527、化合物

試薬・触媒・溶媒 1

HCID 6342Acetonitrile溶媒

実験手順

{3-[5-(4-Chloro-phenyl)-4-(4-nitro-phenyl)-4,5-dihydro-1H-imidazol-2-yl]-5-methoxymethyl-phenyl}-methanol was prepared from 3-hydroxymethyl-5-methoxymethyl-benzonitrile and 1-(4-chloro-phenyl)-2-(4-nitro-phenyl)-ethane-1,2-diamine in an analogous manner as described in example 35. LR-MS (ES): 452 [(M+H)+], 493 [(M+H+CH3CN)+].

出典と根拠

ORDレコード
ord-fad5553e730742658f10a0b535cf6d78
出典データセット
uspto-grants-2003_09
特許番号
US06617346B1

反応ノート

読み込み中…