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Sodium Chloride → methyl N-{1-[3-(4-methoxyphenyl)phenyl]ethyl}carbamate

HRID 1168033
ノート
印刷プレビュー

反応式

HRID 1168033 の反応式
Br[C:2]1[CH:3]=[C:4]([CH:8]([NH:10][C:11](=[O:14])[O:12][CH3:13])[CH3:9])[CH:5]=[CH:6][CH:7]=1.C(=O)([O-])[O-].[Na+].[Na+].[CH3:21][O:22][C:23]1[CH:28]=[CH:27][C:26](OB(O)O)=[CH:25][CH:24]=1.[Cl-].[Na+]>C(O)C.C1C=CC([P]([Pd]([P](C2C=CC=CC=2)(C2C=CC=CC=2)C2C=CC=CC=2)([P](C2C=CC=CC=2)(C2C=CC=CC=2)C2C=CC=CC=2)[P](C2C=CC=CC=2)(C2C=CC=CC=2)C2C=CC=CC=2)(C2C=CC=CC=2)C2C=CC=CC=2)=CC=1.C1(C)C=CC=CC=1>[CH3:21][O:22][C:23]1[CH:28]=[CH:27][C:26]([C:2]2[CH:3]=[C:4]([CH:8]([NH:10][C:11](=[O:14])[O:12][CH3:13])[CH3:9])[CH:5]=[CH:6][CH:7]=2)=[CH:25][CH:24]=1
参加物実験手順後処理出典と根拠反応ノート

参加物

8

反応物 4

HCID 5234Sodium ChlorideHCID 10340Sodium CarbonateHCID 147699944-Methoxyphenyl boric acidHCID 15483792methyl N-[1-(3-bromophenyl)ethyl]carbamate

生成物 1

HCID 22995022methyl N-{1-[3-(4-methoxyphenyl)phenyl]ethyl}carbamate収率 144.7%

試薬・触媒・溶媒 3

HCID 178418397
HCID 178418397、化合物
触媒
HCID 702Ethanol溶媒
HCID 1140Toluene溶媒

実験手順

1.00 g of methyl N-[1-(3-bromophenyl)ethyl]carbamate, 0.41 g of sodium carbonate in aqueous solution (20 ml) and 0.09 g of tetrakis(triphenylphosphine)palladium (0) were added to toluene (40 ml) under a nitrogen atmosphere. The resulting solution was mixed with 0.59 g of 4-methoxyphenylboric acid in ethanol (20 ml) at room temperature with stirring and refluxed under heating for 2 hours. After the reaction, the reaction solution was cooled to room temperature, poured into saturated aqueous sodium chloride and extracted with ethyl acetate, and the organic layer was dried over anhydrous magnesium sulfate and evaporated under reduced pressure for removal of the solvent. The residue was purified by silica gel column chromatography to give 1.45 g of methyl N-{1-[3-(4-methoxyphenyl)phenyl]ethyl}carbamate as pale yellow crystals. m.p. 117-119° C.

後処理

  1. temperaturerefluxed
  2. temperatureunder heating for 2 hours
  3. customAfter the reaction
  4. extractionextracted with ethyl acetate
  5. dry with materialthe organic layer was dried over anhydrous magnesium sulfate
  6. customevaporated under reduced pressure for removal of the solvent
  7. customThe residue was purified by silica gel column chromatography

出典と根拠

ORDレコード
ord-cc1b09f6628d486b98c69a7e9cfed632
出典データセット
uspto-grants-2003_09
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US06620961B1

反応ノート

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