Oxalyl chloride → HCID 86054523、化合物
反応式
[I:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][OH:9])=[C:4]([O:10][CH2:11][CH2:12][CH3:13])[CH:3]=1.C(Cl)(=O)C(Cl)=O>CS(C)=O>[I:1][C:2]1[CH:7]=[CH:6][C:5]([CH:8]=[O:9])=[C:4]([O:10][CH2:11][CH2:12][CH3:13])[CH:3]=1参加物
4
実験手順
The procedure is the same as that described above, using 5.5 g, that is 18.8 mmol, of (4-iodo-2-propoxyphenyl)methanol, 1.8 ml of oxalyl chloride and 3 ml of DMSO. After evaporation of the solvents, 5.5 g (100%) of the expected compound are recovered in the form of a yellow solid.
後処理
- customAfter evaporation of the solvents, 5.5 g (100%) of the expected compound
- customare recovered in the form of a yellow solid
出典と根拠
- ORDレコード
- ord-bdfa82decdb048e99081fb8e363156a0
- 出典データセット
- uspto-grants-2010_11
- 特許番号
- US07829588B2
反応ノート
読み込み中…