4-(Thiophen-2-yl)benzoic acid → HCID 57771755、化合物

HRID 1174967

反応式

HRID 1174967 の反応式
[S:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[C:6]1[CH:14]=[CH:13][C:9]([C:10]([OH:12])=O)=[CH:8][CH:7]=1.[CH3:15][N:16]([CH3:31])[CH2:17][CH2:18][N:19]([CH3:30])[C:20]1[S:21][C:22]2[CH:28]=[C:27]([NH2:29])[CH:26]=[CH:25][C:23]=2[N:24]=1>>[CH3:15][N:16]([CH3:31])[CH2:17][CH2:18][N:19]([CH3:30])[C:20]1[S:21][C:22]2[CH:28]=[C:27]([NH:29][C:10](=[O:12])[C:9]3[CH:8]=[CH:7][C:6]([C:2]4[S:1][CH:5]=[CH:4][CH:3]=4)=[CH:14][CH:13]=3)[CH:26]=[CH:25][C:23]=2[N:24]=1

参加物

3

反応物 2

HCID 7364984-(Thiophen-2-yl)benzoic acidHCID 55226563N2-(2-Dimethylamino-ethyl)-N2-methyl-benzothiazole-2,6-diamine

生成物 1

HCID 57771755HCID 57771755、化合物

実験手順

The title compound is prepared by following General Method A, using 4-thiophen-2-yl-benzoic acid (0.098 g, 0.48 mmol), and N*2*-(2-dimethylamino-ethyl)-N*2*-methyl-benzothiazole-2,6-diamine (0.10 g, 0.40 mmol) to afford the title compound as a white solid. LC/MS: Retention time=4.37 min; (m/z): calcd for C23H24N4OS2 (M+H)+: 437.6; found: 437.3.

後処理

  1. customThe title compound is prepared

出典と根拠

ORDレコード
ord-a38f28e84e2a4225ba11329854baad27
出典データセット
uspto-grants-2010_11
特許番号
US07838543B2

関連ノート

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