関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | (E)-1,3-Dichloropropene | HCID 24726 | — |
| 反応物 | N-Methyl-N-naphthylmethylamine | HCID 84474 | — |
| 溶媒 | Methyl Ethyl Ketone | HCID 6569 | — |
| 生成物 | (E)-3-Chloro-N-methyl-N-(1-naphthylmethyl)-2-propen-1-amine | HCID 9834733 | — |
反応手順
30 g (0.175 mol) N-methyl-1-naphthalene methanamine, 100 ml MEK and 29 g (0.210 mol, 1.2 eq.) potassium carbonate are introduced into a reactor, the mixture is heated to 50° C. and 22.4 g (0.202 mol, 1.1 eq.) of (1E)-1,3-dichloro-1-propene added dropwise.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US07838704B2 |
|---|
| 出典データセット | uspto-grants-2010_11 |
|---|
| ORD ID | ord-449e0bb65a6b42839560eb577a526773 |
|---|
| 出典メモ | uspto-grants-2010_11 |
|---|
