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HRID1175201

反应详情

EQUATION

反应方程式

HRID 1175201 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：Cl/C=C/CCl
HCID24726

trans-1,3-Dichloropropene

C3H4Cl2

结构：CNCc1cccc2ccccc12
HCID84474

N-Methyl-N-naphthylmethylamine

C12H13N

PRODUCTS

生成物

1
结构：CN(C/C=C/Cl)Cc1cccc2ccccc12
HCID9834733

(E)-N-(3-Chloroallyl)-N-methyl-N-(naphthalene-1-yl-methyl)-amine

C15H16ClN

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCC(C)=O
溶剂HCID6569

Methyl ethyl ketone

C4H8O

CONDITIONS

反应条件

温度
50 °C

PROCEDURE

实验过程

30 g (0.175 mol) N-methyl-1-naphthalene methanamine, 100 ml MEK and 29 g (0.210 mol, 1.2 eq.) potassium carbonate are introduced into a reactor, the mixture is heated to 50° C. and 22.4 g (0.202 mol, 1.1 eq.) of (1E)-1,3-dichloro-1-propene added dropwise.