Trifluoroacetic acid → Methyl-phenyl-carbamic Acid 4-[2-(4-imidazol-1-yl-phenoxy)-ethyl]-phenyl Ester
反応式
C(O)(C(F)(F)F)=O.[OH:8][CH2:9][CH2:10][C:11]1[CH:16]=[CH:15][C:14]([O:17][C:18](=[O:27])[N:19]([CH3:26])[C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=2)=[CH:13][CH:12]=1.[N:28]1([C:33]2[CH:38]=[CH:37][C:36](O)=[CH:35][CH:34]=2)[CH:32]=[CH:31][N:30]=[CH:29]1>>[N:28]1([C:33]2[CH:38]=[CH:37][C:36]([O:8][CH2:9][CH2:10][C:11]3[CH:12]=[CH:13][C:14]([O:17][C:18](=[O:27])[N:19]([CH3:26])[C:20]4[CH:21]=[CH:22][CH:23]=[CH:24][CH:25]=4)=[CH:15][CH:16]=3)=[CH:35][CH:34]=2)[CH:32]=[CH:31][N:30]=[CH:29]1参加物
4
実験手順
The title compound was prepared as its TFA salt in 62% yield as an oil using methyl-phenyl-carbamic acid 4-(2-hydroxy-ethyl)-phenyl ester and 4-imidazol-1-yl-phenol.