1-Amino-2-propanol → HCID 131731251、化合物

HRID 1190787

反応式

HRID 1190787 の反応式
[CH3:1][CH2:2][CH2:3][CH2:4][O:5][P:6]([O:13][CH2:14][CH2:15][CH2:16][CH3:17])([O:8][CH2:9][CH2:10][CH2:11][CH3:12])=[O:7].[CH3:18][CH:19]([OH:22])[CH2:20][NH2:21]>>[CH3:12][CH2:11][CH2:10][CH2:9][O:8][P:6]([O:5][CH2:4][CH2:3][CH2:2][CH3:1])([O:13][CH2:14][CH2:15][CH2:16][CH3:17])=[O:7].[CH3:18][CH:19]([OH:22])[CH2:20][NH2:21]

参加物

3

反応物 2

HCID 41-Amino-2-propanolHCID 31357Tributyl Phosphate

生成物 1

HCID 131731251HCID 131731251、化合物

実験手順

Reaction of TBPA with MIPA gives an TBPA/MIPA adduct. TBPA is sold in commerce by Albermarle as Saytex® RB-49. MIPA is sold in commerce by Dow Chemical. 44.8 mmol of TBPA is added to a round bottom flask with 50.74 grams of ethanol. The mixture is heated to reflux after which 44.8 mmol of MIPA is added dropwise and the solution refluxed for 1 hour. The ethanol is removed using a rotary evaporator to produce a yellow crystalline solid.

出典と根拠

ORDレコード
ord-d6ca116be7344af0ad32793e54d9c541
出典データセット
uspto-grants-2014_03
特許番号
US08679990B2

関連ノート

読み込み中…